Fred J. Matthews

Organic Lab Schedule


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1st Semester Organic Lab Schedule - CHEM 3511

2nd Semester Organic Lab Schedule - CHEM 3521

1st Summer Session Organic Lab Schedule - CHEM 3511

2nd Summer Session Organic Lab Schedule - CHEM 3521

Organic Lab Syllabus

Writing the Lab Notebook


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Organic Chemistry

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1st Semester Organic Lab Schedule - CHEM 3511

·         CH 3511 TENTATIVE LABORATORY SCHEDULE - FALL 2009

·         DATE (Tu & Th)
TITLE

·         Sept 1 & 3
Introduction to Organic Lab

·         Sept 8 & 10
Recrystallization of Benzoic Acid

·         Sept 15 & 17
Recrystallization of Benzoic Acid (con't)

·         Sept 22 & 24
Benzoic Acid Analysis - MP and Spectroscopy

·         Sept 29 & Oct 1
Simple Distillation of a Volatile Liquid with a Nonvolatile Impurity

·         Oct 6 & 8
Fractional Distillation with a Packed Column

·         Oct 13 & 15
Distillate Analysis - Micro-Boiling Point, Refractive Index, GLC

·         Oct 27 & 22
GCMS and IR Lecture

·         Nov 3 & Oct 29
GCMS and IR Lecture - Distillate Analysis - GCMS and IR spectra

·         Nov 10 & 5
NMR Lecture

·         Nov 17 & 12
NMR Lecture

·         Nov 24 & 19
NMR Lecture - Introduction to Bruker AC-250

·         Dec 1 & 3
NMR Lecture - Distillate Analysis - PMR spectra

·         Dec 8 (all classes meet on Tuesday)
NMR Lecture - Distillate Analysis
Lab Exam - Check Out


2nd Semester Organic Lab Schedule - CHEM 3521

·         CH 3521 TENTATIVE LABORATORY SCHEDULE - SPRING 2010

·         DATE
TITLE

·        Jan  19
Writing the Lab Notebook in 2nd Semester Organic Lab

·       Jan  26
Cyclohexanol to Cyclohexene - Reaction

·         Feb 2
Cyclohexanol to Cyclohexene - Distillation and Analysis

·         Feb 9
Cyclohexanol to Cyclohexene - Analysis Continued and Spectroscopic Analysis

·         Feb 16
Cyclohexanol to Cyclohexene - Spectroscopic Analysis Continued

·         Feb 23
t-Butyl Alcohol to t-Butyl Chloride - Reaction

·         Mar 2
t-Butyl Alcohol to t-Butyl Chloride - Distillation and Analysis

·         Mar 16
t-Butyl Alcohol to t-Butyl Chloride - Analysis Continued and Spectroscopic Analysis

·         Mar 23
t-Butyl Alcohol to t-Butyl Chloride - Spectroscopic Analysis Continued

·         Mar 30
Fischer Esterification - Reaction

·         April 6
Fischer Esterification - Distillation and Analysis

·         April 13
Fischer Esterification - Analysis Continued and Spectroscopic Analysis

·         April 20
Fischer Esterification - Spectroscopic Analysis Continued

·         April 27
Fischer Esterification - Spectroscopic Analysis Continued

·         Lab Exam - Check Out
    8:00 Tuesday lab - 8:00-10:00 - April 30 - Friday
    11:10 Tuesday lab - 10:30-12:30 - May 3 - Monday
    2:20 Tuesday lab - 1:30-3:30 - May 4 - Tuesday


1st Summer Session Organic Lab Schedule - CHEM 3511

·         CH 3511 TENTATIVE LABORATORY SCHEDULE - SUMMER 2005

·         DATE
TITLE

·         June 6
Introduction to Organic Lab

·         June 7
Recrystallization of Benzoic Acid

·         June 8
Recrystallization of Benzoic Acid (con't)

·         June 9
Benzoic Acid Analysis - MP

·         June 14
Simple Distillation of a Volatile Liquid with a Nonvolatile Impurity

·         June 15
Fractional Distillation with a Packed Column

·         June 16
Distillate Analysis - Micro-Boiling Point, Refractive Index, GLC

·         June 21
Cyclohexanol to Cyclohexene - Reaction

·         June 22
Cyclohexanol to Cyclohexene - Distillation and Analysis

·         June 23
Cyclohexanol to Cyclohexene - Analysis Continued

·         June 28
t-Butyl Alcohol to t-Butyl Chloride - Reaction

·         June 29
t-Butyl Alcohol to t-Butyl Chloride - Distillation and Analysis

·         June 30
t-Butyl Alcohol to t-Butyl Chloride - Analysis Continued

·         July 5
Polarimetry

·         July 6
Complete Labs and Final Exam


2nd Summer Session Organic Lab Schedule - CHEM 3521

·         CH 3521 TENTATIVE LABORATORY SCHEDULE - SUMMER 2010