Fred J. Matthews

Organic Lab Schedule


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1st Semester Organic Lab Schedule - CHEM 3511

2nd Semester Organic Lab Schedule - CHEM 3521

1st Summer Session Organic Lab Schedule - CHEM 3511

2nd Summer Session Organic Lab Schedule - CHEM 3521

Organic Lab Syllabus

Writing the Lab Notebook


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Organic Chemistry

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1st Semester Organic Lab Schedule - CHEM 3511

·         CH 3511 TENTATIVE LABORATORY SCHEDULE - FALL 2007

·         DATE
TITLE

·         Aug 28
Introduction to Organic Lab

·         Sept 4
Recrystallization of Benzoic Acid

·         Sept 11
Recrystallization of Benzoic Acid (con't)

·         Sept 18
Benzoic Acid Analysis - MP and Spectroscopy

·         Sept 25
Simple Distillation of a Volatile Liquid with a Nonvolatile Impurity

·         Oct 2
Fractional Distillation with a Packed Column

·         Oct 9
Distillate Analysis - Micro-Boiling Point, Refractive Index, GLC

·         Oct 23
GCMS and IR Lecture

·         Oct 30
GCMS and IR Lecture - Distillate Analysis - GCMS and IR spectra

·         Nov 6
NMR Lecture

·         Nov 13
NMR Lecture

·         Nov 20
NMR Lecture - Introduction to Bruker AC-250

·         Nov 27
NMR Lecture - Distillate Analysis - PMR spectra

·         Dec 4
NMR Lecture - Distillate Analysis
Lab Exam - Check Out


2nd Semester Organic Lab Schedule - CHEM 3521

·         CH 3521 TENTATIVE LABORATORY SCHEDULE - SPRING 2007

·         DATE
TITLE

·        Jan  16
Writing the Lab Notebook in 2nd Semester Organic Lab

·       Jan  23
Cyclohexanol to Cyclohexene - Reaction

·         Jan 30
Cyclohexanol to Cyclohexene - Distillation and Analysis

·         Feb 6
Cyclohexanol to Cyclohexene - Analysis Continued and Spectroscopic Analysis

·         Feb 13
Cyclohexanol to Cyclohexene - Spectroscopic Analysis Continued

·         Feb 20
t-Butyl Alcohol to t-Butyl Chloride - Reaction

·         Feb 27
t-Butyl Alcohol to t-Butyl Chloride - Distillation and Analysis

·         Mar 13
t-Butyl Alcohol to t-Butyl Chloride - Analysis Continued and Spectroscopic Analysis

·         Mar 20
t-Butyl Alcohol to t-Butyl Chloride - Spectroscopic Analysis Continued

·         Mar 27
Fischer Esterification - Reaction

·         April 2
Fischer Esterification - Distillation and Analysis

·         April 10
Fischer Esterification - Analysis Continued and Spectroscopic Analysis

·         April 17
Fischer Esterification - Spectroscopic Analysis Continued

·         April 24
Fischer Esterification - Spectroscopic Analysis Continued

·         8:00 Tuesday lab - 8:00-10:00 - April 30 - Monday
12:45 Tuesday lab - 10:30-12:30 - May 1 - Tuesday
Lab Exam and Check Out 


1st Summer Session Organic Lab Schedule - CHEM 3511

·         CH 3511 TENTATIVE LABORATORY SCHEDULE - SUMMER 2005

·         DATE
TITLE

·         June 6
Introduction to Organic Lab

·         June 7
Recrystallization of Benzoic Acid

·         June 8
Recrystallization of Benzoic Acid (con't)

·         June 9
Benzoic Acid Analysis - MP

·         June 14
Simple Distillation of a Volatile Liquid with a Nonvolatile Impurity

·         June 15
Fractional Distillation with a Packed Column

·         June 16
Distillate Analysis - Micro-Boiling Point, Refractive Index, GLC

·         June 21
Cyclohexanol to Cyclohexene - Reaction

·         June 22
Cyclohexanol to Cyclohexene - Distillation and Analysis

·         June 23
Cyclohexanol to Cyclohexene - Analysis Continued

·         June 28
t-Butyl Alcohol to t-Butyl Chloride - Reaction

·         June 29
t-Butyl Alcohol to t-Butyl Chloride - Distillation and Analysis

·         June 30
t-Butyl Alcohol to t-Butyl Chloride - Analysis Continued

·         July 5
Polarimetry

·         July 6
Complete Labs and Final Exam


2nd Summer Session Organic Lab Schedule - CHEM 3521

·         CH 3521 TENTATIVE LABORATORY SCHEDULE - SUMMER 2006